Rapid and sensitive method for the determination of propylene oxide in cigarette mainstream smoke by gas chromatography-mass spectrometry.

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Abstrakt

Tytuł:: Rapid and sensitive method for the determination of propylene oxide in cigarette mainstream smoke by gas chromatography-mass spectrometry.
Autorzy:: Diekmann J; Philip Morris Research Laboratories GmbH, Fuggerstr. 3, D-51149 Koeln, Germany. />Douda M
Rustemeier K
Źródło:: Journal of chromatographic science [J Chromatogr Sci] 2006 Jan; Vol. 44 (1), pp. 32-4.
Typ publikacji:: Journal Article
Język:: English
Imprint Name(s):: Publication: <2012- > : Oxford : Oxford University Press
Original Publication: Niles Il : Preston Technical Abstracts
MeSH Terms:: Nicotiana*
Epoxy Compounds/*analysis
Gas Chromatography-Mass Spectrometry/*methods
Smoke/*analysis
Reference Standards ; Sensitivity and Specificity
Substance Nomenclature:: 0 (Epoxy Compounds)
0 (Smoke)
Y4Y7NYD4BK (propylene oxide)
Entry Date(s):: Date Created: 20060408 Date Completed: 20060526 Latest Revision: 20231213
Update Code:: 20240104
DOI:: 10.1093/chromsci/44.1.32
PMID:: 16599409
: Czasopismo naukowe

A rapid method using gas chromatography-mass spectrometry for the analysis of propylene oxide in cigarette mainstream smoke is reported. Validation data show the method, which requires a minimum of sample preparation, to be selective, sensitive, reliable, and robust. Propylene oxide is found in the University of Kentucky Reference Cigarettes 1R4F and 2R4F at concentrations of 0.93 and 0.65 microg/cigarette, respectively, with a quantitation limit of 0.135 microg/cigarette.

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