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Tytuł pozycji:

One-pot synthesis of fluorescent nitrogen and sulfur-carbon quantum dots as a sensitive nanosensor for trimetazidine determination.

Tytuł:
One-pot synthesis of fluorescent nitrogen and sulfur-carbon quantum dots as a sensitive nanosensor for trimetazidine determination.
Autorzy:
Belal F; Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Mansoura University, Mansoura, Egypt.
Mabrouk M; Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Tanta University, Tanta, Egypt.
Hammad S; Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Tanta University, Tanta, Egypt.
Barseem A; Pharmaceutical Analysis Department, Faculty of Pharmacy, Menoufia University, Egypt.
Ahmed H; Pharmaceutical Analysis Department, Faculty of Pharmacy, Menoufia University, Egypt.
Źródło:
Luminescence : the journal of biological and chemical luminescence [Luminescence] 2021 Sep; Vol. 36 (6), pp. 1435-1443. Date of Electronic Publication: 2021 Jun 03.
Typ publikacji:
Journal Article
Język:
English
Imprint Name(s):
Original Publication: Chichester, Sussex, UK : Wiley & Sons, c1999-
MeSH Terms:
Quantum Dots*
Trimetazidine*
Carbon ; Humans ; Nitrogen ; Sulfur
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Contributed Indexing:
Keywords: fluorescent nanosensor; heteroatom-doped carbon quantum dots; plasma; trimetazidine
Substance Nomenclature:
70FD1KFU70 (Sulfur)
7440-44-0 (Carbon)
N762921K75 (Nitrogen)
N9A0A0R9S8 (Trimetazidine)
Entry Date(s):
Date Created: 20210513 Date Completed: 20210908 Latest Revision: 20210908
Update Code:
20240105
DOI:
10.1002/bio.4083
PMID:
33982840
Czasopismo naukowe
Water-soluble and highly stable N,S-doped CQDs (N,S-CQDs) were synthesized using a low-cost strategy with citric acid and thiosemicarbazide in one step for use as a fluorescent nanosensor. The achieved N,S-CQDs produced strong emission at 446 nm upon excitation at 370 nm and a high quantum yield of 58.5%. The quenching effect on the prepared N,S-CQDs was utilized for determination of trimetazidine (TMZ) spectrofluorimetrically over a wide linear range 0.04-0.5 μM (0.0106-0.133 μg ml -1 ) and a low limit of detection of 0.01 μM (0.002 μg ml -1 ). Furthermore, CDs were used as a simple and rapid fluorescent probe to determine TMZ in its pharmaceutical formulations as well as in human plasma. The method was tested in compliance with International Council for Harmonisation guidelines. The results obtained were compared statistically with those given for a reported method showing no significant variation regards accuracy and precision.
(© 2021 John Wiley & Sons, Ltd.)

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