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Title of the item:

Structure and spectroscopic properties of N,S-coordinating 2-methylsulfanyl-N-[(1H-pyrrol-2-yl)methylidene]aniline methanol monosolvate.

Title :
Structure and spectroscopic properties of N,S-coordinating 2-methylsulfanyl-N-[(1H-pyrrol-2-yl)methylidene]aniline methanol monosolvate.
Authors :
Richards, D. Douglas
Ang, M. Trisha C.
McDonald, Robert
Bierenstiel, Matthias
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Subject Terms :
CRYSTAL structure
IMINES
HYDROGEN bonding
Source :
Acta Crystallographica: Section E (International Union of Crystallography - IUCr); 2015, Vol. 71 Issue 10, p1136-1139, 8p
Academic Journal
The reaction of pyrrole-2-carboxaldehyde and 2-(methylsulfanyl)aniline in refluxing methanol gave an olive-green residue in which yellow crystals of the title compound, C12H12N2S∙CH3OH, were grown from slow evaporation of methanol at 263 K. In the crystal, hydrogen-bonding interactions link the aniline molecule and a nearby methanol solvent molecule. These units are linked by a pair of weak C-H⋯Omethanol interactions, forming inversion dimers consisting of two main molecules and two solvent molecules. [ABSTRACT FROM AUTHOR]
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