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Title of the item:

Jet Milling as an Alternative Processing Technique for Preparing Polysulfone Hard Nanocomposites

Title :
Jet Milling as an Alternative Processing Technique for Preparing Polysulfone Hard Nanocomposites
Authors :
Amaia Llorente
Berna Serrano
Juan Baselga
Gabriel Gedler
Rahmi Ozisik
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Subject Terms :
Materials of engineering and construction. Mechanics of materials
TA401-492
Source :
Advances in Materials Science and Engineering, Vol 2019 (2019)
Publisher :
Hindawi Limited, 2019.
Publication Year :
2019
Collection :
LCC:Materials of engineering and construction. Mechanics of materials
Document Type :
article
File Description :
electronic resource
Language :
English
ISSN :
1687-8434
1687-8442
Relation :
https://doaj.org/toc/1687-8434; https://doaj.org/toc/1687-8442
DOI :
10.1155/2019/3501402
Access URL :
https://doaj.org/article/34c5f4174faf4c9a869097495ae1027b
Accession Number :
edsdoj.34c5f4174faf4c9a869097495ae1027b
Academic Journal
This work describes how a solid-state blending method such as jet milling can be used to successfully prepare polysulfone (PSU)/γ-alumina nanocomposites. For comparison purposes, conventional melt extrusion was used as well. Morphological analysis revealed how jet mill blending allows obtaining well-dispersed γ-alumina nanoparticles within a polysulfone matrix without any surface treatment, with an important decrease of particle size promoted by the breakup of agglomerates and aggregates due to the particle-particle impacts during processing, which was not observed in the extruded nanocomposites. DSC analysis demonstrated that jet-milling processing promoted Tg enhancements with alumina addition, while TGA experiments confirmed the increment of thermal stability of the nanocomposites prepared by jet milling when compared with the composites prepared by extrusion. The tensile tests showed that ductility remains at a high value for milled nanocomposites, which agreed with the fracture surface images revealing large plastic deformation as a function of the alumina content. This comparative study indicates that the dispersion of nanoparticles in PSU was more homogeneous, with smaller nanoparticles when preparing nanocomposites using jet milling, showing a strong correlation with the enhanced final properties of the nanocomposites.
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